Submitted two plates for sequencing. Each sample two times from each direction.
PCR – Two new Dungan isolates
Repeat of yesterday’s PCR, but with AmpliTaq, less gDNA and 50uL rxn volume. PCR set up is here.
Gel loaded and run by Steven. Not entirely sure of the loading order. However, it doesn’t really matter…
Results: Still absolutely nothing.
UPDATE: Noticed on 20090713 that the reactions didn’t have dNTPs. Probably explains why it didn’t work!
qPCR – Rab7_SYBR primers on abalone RNA and DNased RNA
Attempt to find out if gDNA contamination exists iafter Ambion treatment. Previous test (on 20090414) suggests the QT Kit did not eliminate gDNA. PCR set up and plate layout here. Used Immomix and SYTO 13.
PCR – Two new Dungan isolates from earlier today
Set up PCRs on:
MIE-14y
VNTc-1.2-C1/G10
Used Euk A/B and LABY A/Y primers. Anneal temp 50C. PCR set up is here.
NOTE: Due to the extremely low concentrations of gDNA from these two samples, I used a large amount of gDNA in the rxns. Check the PCR set up link for actual numbers.
Lane 1 – Hyperladder (5uL)
Lane 2 – VNTc-1.2-C1/G10 (Euk primers)
Lane 3 – MIE-14y (Euk primers)
Lane 4 – H2O (Euk primers)
Lane 5 – H2O (Euk primers)
Lane 6 – VNTc-1.2-C1/G10 (Laby primers)
Lane 7 – MIE-14y (Laby primers)
Lane 8 – H2O (Laby primers)
Lane 9 – H2O (Laby primers)
lane 10 – 100bp Ladder
Results: Nada. Probably because of low [gDNA], but could also be due to PCR inhibitors in the gDNA. Will retry using Amplitaq and less gDNA.
gDNA Isolation – Two new Dungan isolates
Isolated gDNA from the following two samples:
MIE-14y
VNTc-1.2-C1/G10
Samples were spun @ 16,000g @ RT for 2mins. No visible pellets in either sample. EtOH was removed. “Pellets” were washed in 1x PBS (pH=7.6) two times and then the Qiagen DNEasy Kit protocol was followed. Samples were incubated @ 55C with Proteinase K for ~2hrs.
Results: Both samples show really, really low quantities of gDNA.
PCR – Test QT Kit with No RT Abalone rxns from 20090408
Anneal 55C. PCR set up is here (bottom half of sheet).
Lane 1 – Hyperladder
Lane 2 – gDNA
Lane 3 – cDNA pool
Lane 4 – No RT 06:5-31
Lane 5 – No RT 06:6-43
Lane 6 – No RT 08:3-5
Lane 7 – No RT 08:3-6
Lane 8 – No RT 08:3-7
Lane 9 – H2O
Lane 10 – H2O
Lane 11 – 100bp ladder
Results: No signal in the gDNA. Appropriate sized band in cDNA pool. Nothing in the water samples. HOWEVER, got bands in tow of the “No RT” rxns (08:3-6/7)!! It’s odd that the gDNA didn’t produce any signal, but there shouldn’t be any signal in the No RT rxns. This indicates gDNA contamination. Should have also tested RNA and DNased RNA. Will test these in order to determine if that system is better at eliminating gDNA carryover.
PCR – Bay/Sea scallop gDNAs
Used higher annealing temps to improve primer specificity, compared to yesterday’s results. PCR set up and plate layout is here.
See the PCR/plate set up link for samples. Hyperladder is placed between every 12 samples.
Results: See this Google Spreadsheet for a summary of the 4 gels from the last two days.
PCR – Bay/Sea scallop gDNA isolated earlier today
Used 3 sets of reverse primers:
Bay_Actin_Rv0
Bay_Actin_Rv2
Sea_Actin_Rv2
Primers were slected based on information from Steven’s notebook (#8, 12/30/2007-1/3/2008). Anneal temp 53C.
PCR set up here . Plate layout here .
Samples were run out by Steven the following day.
Gel 1 of 3
Gel 2 of 3
Gel 3 of 3
Results:
gDNA Isolation – Bay/Sea Scallop and hybrid samples
gDNA was isolated using 500uL of 10% Chelex. Samples were heated @ 95C for 1hr w/periodic vortexing. Samples were then spun 16,000g for 5mins @ 4C. Stored @ -20C in Bay x Sea Scallop Project Box.
PCR – Abalone gDNA/RNA/cDNA w/new TOLLIP primer
Performed a new PCR on the three types of samples listed above with new TOLLIP primers. The new TOLLIP primers (H.discus_806_F/Ab_866_Rv) surround a putative intron. Thus, they will be useful for determining the presence of gDNA contamination in RNA/cDNA. Anneal temp 55C. PCR set up is here .
Lane 1 – Hyperladder
Lane 2 – gDNA
Lane 3 – cDNA (QT)
Lane 4 – RNA (untreated)
Lane 5 – DNased RNA
Lane 6 – QT Kit, No RT
Lane 7 – H2O
Lane 8 – H2O
Results: This could possibly be the most confusing gel I’ve ever had the “pleasure” of running/analyzing, despite that it only has 7 samples.
No band in the gDNA sample, which could be explained by the intron size being too large for amplification with a basic polymerase. The cDNA worked as expected and contains a band of ~150bp. The RNA sample has a faint band of ~750bp. The DNased RNA sample has a band of ~400bp. The differences seen betweeen the gDNA (Lane 2), RNA (Lane 4) and DNased RNA (Lane 5) are truly bizarre. The No RT sample has no band. And, to top things off, one of the H2O samples is blank , but the other one has a band of ~1500bp! Ugh. How is all of this even possible?